Main > PHARMA. > Quinolinone. > FloseQuinan. > Halogenated FloseQuinan. > Chlorinated FloseQuinan > MonoChloro FloseQuinan. > Patent. > Claims Etc > Claim 1: Racemic ChloroFloseQuinan > Claim 2: (S)-(+)-ChloroFloseQuinan > in Enantiomeric Excess. Claims 3,4: > (S)-(+)-FloseQuinan in > 90,95% > resp. ee. Claim 5: > R)-(-)-FloseQuinan in ee. Claims 6, > 7: R)-(-)-FloseQuinan in 90,95% > resp. in ee. Claim 8: > 3-Cl-Me-Sulfonyl-7-F-1-Me-4-Quinolo > ne. Claim 9: 3-Cl-Me-Thio-7-F-1-Me- > 4-Quinolone. Claim 10: > ChloroDesOxyFloseQuinan Synthesis > b) FloseQuinan+(Ph)3P Reaction= > DesOxyFloseQuinan (D) > (7-F-1-Me-3-Me-Thio-4-Quinolone) in > Org. Solv.; c) (D)+N-Cl-Succinimide > +2,2-AzoBisIsobutyroNitrile= > ChloroDesOxyFloseQuinan (C) > (3-Cl-Me-Thio-7-F-1-Me-4-Quinolone) > in Org. Solv. Claim 11: (b) Solv. > Select: CCl4 Etc. Claim 15: > (c) Solv. Select: CCl4 Etc. Claim > 17: MonoChloroFloseQuinan Synthesis > : ChloroDesOxyFloseQuinan+H2O2+ > K2CO3 in CCl4 Solv. Reaction.

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