Main > ORGANIC CHEMICALS > Aliphatics > Acids > DiAcids > Adipic Acid > Mfg > Cyclohexane Oxidation > Catalyst Removal

Product USA. T

PATENT ASSIGNEE'S COUNTRY USA
UPDATE 06.99
PATENT ASSIGNEE This data is not available for free
PATENT CLAIMS Method of removing catalyst from reaction mixt contg adipic acid, the reaction mixt having been formed after reaction of cyclohexane with an oxidant in presence of catalyst, water & AcOH solvent, in an oxidation zone, comprising
- Precipitating part of catalyst in first catalyst precipitation
zone by removing water at least partially from reaction
mixt &/or controlling T to be adequately high for causing
partial catalyst precipitation
- Removing the precipitated catalyst, thus forming a second
mother liquor comprising dissolved catalyst, AcOH solvent
& adipic acid
- Removing partially AcOH solvent & melting adipic acid
until catalyst precipitates in second catalyst precipitation
zone
- Removing the precipitated catalyst
PATENT PHOTOCOPY Available on request

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