Main > ORGANIC CHEMICALS > Aromatics > Acids > Liquid Phase. Mfg > AcOH Reaction Solvent

Product Japan. MMT

PATENT ASSIGNEE'S COUNTRY Japan
UPDATE 09.99
PATENT ASSIGNEE This data is not available for free
PATENT CLAIMS - Subjecting alkyl-substituted aromatic compd to liquid phase
oxidation with O2 in AcOH as solvent in presence of catalyst
- Producing water-contg AcOH by cooling & condensing an
exhaust gas from the oxidation reactor
- Dehydrating said water-contg AcOH by azeotropic distn
in tower
- Feeding an entrainer to top portion of azeotropic distn tower
to suppress the concn of alkyl-substituted aromatics in
entrainer to concn < 10%
- Recycling to oxidation reactor the resultant dehydrated
AcOH as solvent
PATENT PHOTOCOPY Available on request

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