Main > ORGANIC CHEMICALS > Aliphatics > CycloAliphatics. > Hexanol. + Hexanone

Product USA. D. No. 1

PATENT ASSIGNEE'S COUNTRY USA
UPDATE 04.99
PATENT ASSIGNEE This data is not available for free
PATENT CLAIMS Mfg process by cyclohexane air oxidation
- Reacting cyclohexane with air to produce first mixt compri
sing cyclohexanol (I), cyclohexanone (II), cyclohexylhydro
peroxide (III) & cyclohexane (IV)
- Reacting (III) with aq caustic to produce second mixt compri
sing organic phase of (I), (II) & (IV) & aq phase of water &
caustic
- Sepg aq/organic phases of second mixt
- Contacting organic phase with water (including polyprotic
acid capable of neutralizing caustic & forming buffer pH 7
- 9.5) to extract portion of caustic
- Distilling organic phase to separate (IV) from (I) & (II)
Whereby oligomerization of (II) is eliminated
PATENT PHOTOCOPY Available on request

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