Main > ORGANIC CHEMICALS > Aromatics > Acids > DiAcid > Terephthalic. Isophthalic. Acid > Carboxybenzaldehyde Redn

Product USA. H.

PATENT ASSIGNEE'S COUNTRY USA
UPDATE 07.99
PATENT ASSIGNEE This data is not available for free
PATENT CLAIMS Method for reducing 4-CBA in TPA production or 3-CBA in isophthalic acid production comprising
- Dissolving crude TPA (or crude IPA) in solvent at 50-250C
to form soln
- Crystallizing purified acid from soln by reducing the T &/or
pressure
- Separating said crystallized purified TPA from soln
- Adding an oxidant to CBA oxidizer to oxidize said filtered
soln in (previous step) causing 4-CBA (or 3-CBA) to con
vert to TPA (or IPA)
- Evaporating solvent from soln
- Cooling concentrated soln to crystallize additional purified
TPA & filtering said slurry
- Recycling major portion of mother liquor from previous step
to dissolver in first step & minor portion of mother liquor
from previous step to a purge stream
PATENT PHOTOCOPY Available on request

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