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Product Acetic Anhydride. Mfg. USA. E.

PATENT ASSIGNEE'S COUNTRY USA
UPDATE 07.99
PATENT ASSIGNEE This data is not available for free
PATENT CLAIMS - Continuously feeding to first reaction zone MeOAc (I), MeI
(II), Dissolved catalyst comp. comprising rhodium & promo
ters (III), AcOH solvent (IV) & CO, wherein CO is fed below
surface of liquid reaction mixt to produce first liquid reaction
mixt comprising (I), (II), (III), (IV), dissolved CO & acetic anhy
dride product
- Feeding first liquid reaction mixt from first to second reaction
zone comprising reaction vessel in which is maintained a
liquid phase comprising first liquid reaction mixt & an over
head vapor space wherein total pressure 40 - 50 bar absolu
te is maintained, no CO is fed below surface of liquid phase
& residence time is > 2 min to produce second liquid reac
tion mixt comprising (I), (II), (III), (IV), dissolved CO & acetic
anhydride product
- Removing second liquid reaction mixt. from second reac
tion zone
Whereby utilization of CO in process is increased
PATENT PHOTOCOPY Available on request

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