Main > POLYMERS > A - M O N O M E R S > Carbonate Monomer > Di-Aryl Carbonate > Production > Aromatic DiOl > Oxidative Carbonylation Process > Catalyst System > Platinum-group-metal Catalyst > Recovery > Suspension Crystallization

Product DE. B

PATENT ASSIGNEE'S COUNTRY Germany
UPDATE 10.99
PATENT ASSIGNEE This data is not available for free
PATENT CLAIMS Catalyst system comprises Pt-group-metal catalyst, co-catalyst, quat. salt & base. Recovery process comprises steps
(a) The reaction soln is transferred from a reactor for producing di-aryl carbonate into an apparatus suitable for suspension crystallization
(b) The said crystallization is initiated in said apparatus by T redn to form crystallizate
(c) Said crystallizate, which consists mainly od di-aryl carbonate & parent aromatic diol is separated from residual catalyst-contg mother liquor, said separated crystallizate is washed with a water-free wash soln comprising the aromatic diol or mixt of diaryl carbonate & aromatic diol & the wash soln is recycled into the production of diaryl carbonate
(d) Said crystallizate is worked up to pure diaryl carbonate & pure aromatic diol
(e) Said mother liquor is recycled into said reactor for producing diaryl carbonate or is worked up to recover said Pt-group-metal catalyst
PATENT PHOTOCOPY Available on request

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