Main > STEROIDS > Sterol > Tall Oil Pitch. Derived

Product USA. W

PATENT ASSIGNEE'S COUNTRY USA
UPDATE 05.00
PATENT ASSIGNEE Westvaco
PATENT CLAIMS Method for the isolation of sterols from sulfate pulping process tall oil pitch
- Saponifying the said pitch
- Extracting the neutral fraction from saponified pitch
- Blending a hydrocarbon soln of the neutrals with an alc.
solvent at T > crystallization T of sterol to produce a hydro
carbon/neutrals/alc. soln
- Adding water of T > than soln. T to separate into an upper
organic phase & lower alc./water phase
- Removing lower alc./water phase
- Allowing remaining upper phase to cool to 20-30C to
produce sterol crystals
- Recovering said crystals from cooled soln
- Washing said crystals with a hydrocarbon solvent to
obtain sterol yield > 60% & purity > 90%
PATENT PHOTOCOPY Available on request

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